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Its primary applications in the reductive amination of aldehydes and ketones under neutral or mildly acidic reaction conditions. This resin was developed to perform in a manner similar to that of the well-established sodium triacetoxyborohydride, while simplifying reagent handling and product purification. Moreover, for many of these reactions, a scavenger resin may be added for one-pot purification of the product. Our carefully selected portfolio of industrial scale products have a proven track record of successful applications and use in scale-up projects.

We can support the discovery, development and manufacturing of customer pharmaceutical and biotechnology products, from pre-clinical, phase I, II and III to small scale commercial operations. MP-Triacetoxyborohydride has primary applications in the reductive amination of aldehydes and ketones under neutral or mildly acidic reaction conditions.

The resin has primary applications in the reductive amination of Committed to preserving our shared environment — further details available on request. Manufacture of consumables is accredited by the world renowned British Standards Sundbyberg ar rikast i stockholm. Flexible supply chains, back up manufacturing and warehousing ensures supply risk reduction. Long to indefinite product shelf life, reduced process risk.

Supports pharma guidelines for reducing elemental impurities in APIs. Further extractable Sundbyberg ar rikast i stockholm provided on request.

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Raw materials certified free of materials of human or animal origin. Chemical substances used in our manufacturing process do not require registration. Able to withstand mechanical stirring and heating under normal reaction conditions. Download the product note. Sodium triacetoxyborohydride has emerged as one of the reagents used most frequently for carrying out reductive amination of carbonyl compounds, a reaction that is also known as reductive alkylation of amines.

This reagent Sundbyberg ar rikast i stockholm gained preference relative to other reducing agents as a result of its mild reaction conditions and broad scope of reactivity. The typical conditions for reductive amination reactions with sodium triacetoxyborohydride utilize 1. A disadvantage of sodium triacetoxyborohydride is its poor solubility, and that product isolation requires an aqueous quench followed by liquid-liquid extraction and column chromatography.

MP-Triacetoxyborohydride offers scope and reactivity similar to that of sodium triacetoxyborohydride with the additional convenience of a polymer-supported reagent for handling and purification. Typical conditions require 2. Acetic acid is not required Scheme 2. After the reaction is complete, a scavenger resin may be added for product purification.

For example, in the case of reductive alkylation using an excess of primary amine, PS-Benzaldehyde may be used to scavenge the excess starting primary amine from the product secondary amine. Likewise, in the case of reductive alkylation of secondary amines, an excess of the starting secondary amine may be scavenged by PS-Isocyanate.

The product is then isolated by simply filtering off the resins. Sundbyberg ar rikast i stockholm triacetoxyborohydride content of the resin is determined by hydrolyzing the resin with aqueous HCl 1 M. The capacity is calculated based on the amount of liberated hydrogen gas collected. The THF is required to stabilize the resin and it is important not to remove this by drying in vacuo.

Storage of samples for multiple months at room temperature does not affect the resin. A THF solution 0. When the reaction was complete, PS-Benzaldehyde 0. The resin was filtered and washed with THF 2 x 4 mL.

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The secondary amine was characterized by gas chromatography and 1H NMR. For further information please see product note PPS Contact me about this product.

About Part Numbers Technical Specs. Log in for hundreds of free application notes and support documents.

Stockholm, SE37 LISTENERS; Gothenburg, SE24...

Industrial Product Portfolio Our carefully selected portfolio of industrial scale products have a proven track record of successful applications and use in scale-up projects.

BrochuresEnglish Part No: Product Notes Part No: Can be Sundbyberg ar rikast i stockholm in processes in compliance with cGMP standards. Flexible supply chains, back up manufacturing and warehousing ensures supply risk reduction Can be used in processes in compliance with GLP standards. Products which are scaleable from lab or development to process scale. Background Sodium triacetoxyborohydride has emerged as one of the reagents used most frequently for carrying out reductive amination of carbonyl compounds, a reaction that is also known as reductive alkylation of amines.

Capacity and Stability The triacetoxyborohydride content of the resin is determined by hydrolyzing the resin with aqueous HCl 1 M. Log in for price. Starweb AB grundades år och erbjuder en modern, responsiv e- handelsplattform med fokus på försäljning och konvertering. Med mer än Sundbyberg ar rikast i stockholm funktioner.

Established and now operates in Stockholm, Göteborg, Malmö, Uppsala, Är du nyexad eller snart klar med dina studier inom HR/Beteende/System eller.

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Its primary applications in the reductive amination of aldehydes and ketones under neutral or mildly acidic reaction conditions. This resin was developed to perform in a manner similar to that of the well-established sodium triacetoxyborohydride, while simplifying reagent handling and product purification.

Moreover, for many of these reactions, a scavenger resin may be added for one-pot purification of the product. Our carefully selected portfolio of industrial scale products have a proven track record of successful applications and use in scale-up projects.

We can support the discovery, development and manufacturing of customer pharmaceutical and biotechnology products, from pre-clinical, phase I, II and III to small scale commercial operations. MP-Triacetoxyborohydride has primary applications in the reductive amination of aldehydes and ketones under neutral or mildly acidic reaction conditions.

The resin has primary applications in the reductive amination of

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Biotage® MP-Triacetoxyborohydride

After getting a record deal with Universal Music in the early he had a couple of hits on the Swedish radio as the singer Evan. The THF is required to stabilize the resin and it is important not to remove this by drying in vacuo.

A disadvantage of sodium triacetoxyborohydride is its poor solubility, and that product isolation requires an aqueous quench followed by liquid-liquid extraction and column chromatography. Both polypropylene units are equipped with vacuum gauge and fine vacuum controller. Manufacture of consumables is accredited by the world renowned British Standards Institute. Log in for price.

Powerful Supported Triacetoxyborohydride for Reductive Amination

That manifold is ideal when processing well SPE, supported liquid extraction or protein precipitation plates either manually or with an automated liquid handling system.

In this catalog product poop is displayed with easy-to-follow application details and supporting documentation. Ordering information is found following each upshot listing. The method described in this application from Biotage Labs demonstrates alpine, reproducible recovery of teicoplanin from human plasma.

A wide variety of anthology plates can also be used, and cross contamination between wells is minimized by correct use of inserts and spacers in both base and lid, which aid plate positioning. Its lightweight construction allows the lid to beyond be manipulated, and the optional standalone vacuum units mean space need on automation decks is minimized.

The sloping polypropylene base drains waste on the double out of the various base, eliminating the go hungry for a removable become debilitated tray.

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A disadvantage of sodium triacetoxyborohydride is its poor solubility, and that product isolation requires an aqueous quench followed by liquid-liquid extraction and column chromatography. Supports pharma guidelines for reducing elemental impurities in APIs. Products which are scaleable from lab or development to process scale. The secondary amine was characterized by gas chromatography and 1H NMR. About Part Numbers Technical Specs. The product is then isolated by simply filtering off the resins.

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